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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1088523Generated: October 30, 2026

Benzene → HCID 22163151, compound

https://huagongshe.com/reaction/1088523

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzeneHCID 241—
ReactantBenzocaineHCID 2337—
Reactant1-TetraloneHCID 10724—
SolventWaterHCID 962—
ProductHCID 22163151HCID 22163151—

Reaction Steps

A solution of α-tetralone (40 ml), ethyl-p-amino-benzoate (42 g) and benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with the continuous removal of water. The crude product was crystallized from ethanol to give N-(1,2,3,4-tetrahydonaphthylidene)-p-carbethoxyaniline (XXVIII). XXVIII had a.m.p. of 108.5° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04962234
Source datasetuspto-grants-1990_10
ORD IDord-a1e83c5405a94189936c93b85832b6af
Source noteuspto-grants-1990_10