HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 22163151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | 1-Tetralone | HCID 10724 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22163151 | HCID 22163151 | — |
Reaction Steps
A solution of α-tetralone (40 ml), ethyl-p-amino-benzoate (42 g) and benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with the continuous removal of water. The crude product was crystallized from ethanol to give N-(1,2,3,4-tetrahydonaphthylidene)-p-carbethoxyaniline (XXVIII). XXVIII had a.m.p. of 108.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-a1e83c5405a94189936c93b85832b6af |
| Source note | uspto-grants-1990_10 |