HRID1088565

反应详情

EQUATION

反应方程式

HRID 1088565 的结构方程式

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

A mixture of 1.3 g of 1-methyl-1,2,3,4-tetrahydro-2-quinolinemethanol and 1.37 g of methyl p-toluenesulfonate was heated at 100° C. for 6 hours. The solvent was removed from the reaction mixture by decantation, and the residue was washed with ether to give 2.7 g of the desired compound as a dark red oil.

WORKUP

后处理

  1. customThe solvent was removed from the reaction mixture by decantation
  2. washthe residue was washed with ether