Methyl p-toluenesulfonate → HCID 15052266, compound

HRID 1088574Notes

Reaction equation

HRID 1088574 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][CH2:8][OH:9])[CH:2]=1.[C:10]1([CH3:21])[CH:15]=[CH:14][C:13]([S:16]([O:19]C)(=[O:18])=[O:17])=[CH:12][CH:11]=1>>[C:10]1([CH3:21])[CH:11]=[CH:12][C:13]([S:16]([O-:19])(=[O:17])=[O:18])=[CH:14][CH:15]=1.[OH:9][CH2:8][CH2:7][C:3]1[CH:2]=[N+:1]([CH3:10])[CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 6645Methyl p-toluenesulfonateHCID 805153-Pyridineethanol

Product 1

HCID 15052266HCID 15052266, compoundYield 200.1%

Procedure

The procedures of Reference Example 10 were repeated using 1.00 g of 3-pyridinethanol and 1.51 g of methyl p-toluenesulfonate to give 2.51 g of the desired compound.

Sources & evidence

ORD record
ord-da60d7d1e6e440a28e0352dd5eeba5d9
Source dataset
uspto-grants-1990_10
Patent number
US04962096

Reaction notes

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