2-Amino-4,6-dimethoxypyrimidine → HCID 15616170, compound

Participants

Reaction Steps

1.55 g (0.01 mole) of 2-amino-4,6-dimethoxypyrimidine are dissolved in 100 ml of dichloromethane, and 3.40 g (0.012 mole) of allyl 2-isocyanatosulfonyloxybenzoate, dissolved in 20 ml of dichloromethane, are added at 0° C. The mixture is stirred at room temperature for 18 hours and filtered off with suction, and 2.54 g (58% of theory) of allyl 2-[3-(4,6-dimethoxypyrimidin-2-yl)ureidosulfonyloxy]-benzoate of melting point 110°-112° C. are obtained.

Provenance & Evidence