HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22691250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 131716660 | HCID 131716660 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22691250 | HCID 22691250 | — |
Reaction Steps
The hydrochloride product from part (c) (1.61 g., 4.81 mmole) is partitioned between ethyl acetate and 5% aqueous sodium bicarbonate (100 ml. each). The organic layer is separated, washed with brine, dried (MgSO4), and concentrated in vacuo to give 3-[[(S)-2-amino-1-oxo-3-phenylpropyl]amino]benzoic acid, methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963539 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-2d438d2fec2e4dd281120b2c3dcbcb18 |
| Source note | uspto-grants-1990_10 |