HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12228900, compound → 6(2H)-Isoquinolinone, octahydro-2-methyl-, cis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12228900 | HCID 12228900 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6(2H)-Isoquinolinone, octahydro-2-methyl-, cis- | HCID 15663953 | — |
Reaction Steps
2-Methyl-1,2,3,4,6,7,8,8a-octahydroisoquinol-6-one (3.30 g) in ethanol (75 ml) was hydrogenated at 60 p.s.i. in the presence of 5% Pd/C (0.5) for 2.5 hours. The catalyst was filtered off and the filtrate evaporated to give a light brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963558 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-3f40ce1fce8b44ebaa08fc149962a8d9 |
| Source note | uspto-grants-1990_10 |