HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4-Dipropyl-1,1-cyclohexanediacetic acid → HCID 14836346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4-Dipropyl-1,1-cyclohexanediacetic acid | HCID 14836345 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 14836346 | HCID 14836346 | 90% |
Reaction Steps
4,4-Dipropylcyclohexane-1,1 diacetic acid, prepared as described in Example 18, was dissolved in acetic anhydride and refluxed for 1-6h. The excess acetic anhydride was removed by distillation under reduced pressure and the residue was recrystallized form hexanes; m.p. 91-93° ; yield 90-95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963557 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-4f2dccf63d9845d4af61af7c75f86d83 |
| Source note | uspto-grants-1990_10 |