HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12181446, compound → HCID 21806145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12181446 | HCID 12181446 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21806145 | HCID 21806145 | 96.8% |
Reaction Steps
4-(2-Quinolinyl)-3-butynol (2.53 g) was hydrogenated over pre-reduced 10% palladium on charcoal (50% aqueous paste, 0.6 g) in ethanol (100 ml) at room temperature and pressure. The reaction mixture was filtered through hyflo and evaporated in vacuo to afford the title compound as a colourless semi-solid (2.50 g), t.l.c. (diethyl ether), Rf 0.20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963564 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-cd4512de3e3e47dfae4e0eb64ff01501 |
| Source note | uspto-grants-1990_10 |