HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 19756210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 15100972 | HCID 15100972 | — |
| Product | HCID 19756210 | HCID 19756210 | — |
Reaction Steps
A mixture of 2 g of 4-(chloroacetyl)-4,5-dihydro-7-[3-(trifluoromethyl)phenyl]pyrazolo[1,5-a]pyrimidine-3-carbonitrile and 20 ml of concentrated sulfuric acid was stirred at room temperature for 2 hours, then poured into ice water, stirred, and filtered. The product was washed with water and dried giving 2 g of the desired intermediate,. mp 174°-176°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963553 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-f4e43c6639bf414785ae16ee4c4f0730 |
| Source note | uspto-grants-1990_10 |