HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → N-(5-nitro-indan-2-yl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | N-(2,3-Dihydro-1H-inden-2-yl)acetamide | HCID 12452137 | — |
| Product | N-(5-nitro-indan-2-yl)-acetamide | HCID 14820512 | — |
Reaction Steps
20.5 g of 2-acetylaminoindan is added gradually into 200 ml of fuming nitric acid under cooling. After the reaction, the reaction mixture is poured onto 100 g of ice, and the solvent is evaporated from the chloroform extract, and the residue is recrystallized from isopropyl alcohol to give 18.6 g of 2-acetylamino-5-nitroindan.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963587 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-121b83492bf444a3b2d438e6d8c26b8d |
| Source note | uspto-grants-1990_10 |