HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-1-Indanone → HCID 12374669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-1-Indanone | HCID 334036 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12374669 | HCID 12374669 | — |
Reaction Steps
33.5 g (0.2065 mol) of 6-methoxy-2,3-dihydro-1H-indenone is added in portions to a solution of 3.8 g (0.1 mol) of lithium aluminium hydride in 700 ml of dry ether and 50 ml of dry tetrahydrofuran, under an inert atmosphere with cooling. (H.0. House et al. J. Org. Chem. 35 647-51, 1970 and J. Org. Chem. 42, 2155-60, 1977).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963680 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-307fbf7560f942f7a0c7fd561c389752 |
| Source note | uspto-grants-1990_10 |