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HRID1088921

反应详情

EQUATION

反应方程式

HRID 1088921 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CC(=O)Nc1ccc(N=C=S)cc1
HCID2772285

N-(4-isothiocyanatophenyl)acetamide

C9H8N2OS

结构：Nc1ccc2c(c1)NC(=O)CC2
HCID5200242

7-Amino-3,4-dihydro-1H-quinolin-2-one

C9H10N2O

PRODUCTS

生成物

1
结构：CC(=O)Nc1ccc(NC(=S)Nc2ccc3c(c2)NC(=O)CC3)cc1
HCID15719020

未命名化合物

收率 85%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

CONDITIONS

反应条件

温度
20 °C

PROCEDURE

实验过程

A mixture containing 1.92 g of 4-acetamidophenylisothiocyanate and 1.62 g of 7-amino-3,4-dihydro-2(1H)quinolone in 10 ml of DMF was stirred for 6 h at 20° C. Water was added and the product filtered and washed with water. Yield 85%.

WORKUP

后处理

  1. filtrationthe product filtered
  2. washwashed with water