HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22162367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Cyanoindole | HCID 230282 | — |
| Reactant | HCID 22162364 | HCID 22162364 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22162367 | HCID 22162367 | — |
Reaction Steps
To a solution of 1.0 g of 3-cyanoindole in 30 ml of ethyl acetate was added 1.1 ml of diethyldithiophosphonic acid. The solution was then saturated with gaseous hydrogen chloride and stirred at room temperature for 18 hours. The thioamide was isolated from the reaction mixture as a tan precipitate and used directly in the following reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963689 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-8d76ba55745c4dbfb5de77da57ab500e |
| Source note | uspto-grants-1990_10 |