HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 14075318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14075319 | HCID 14075319 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14075318 | HCID 14075318 | — |
Reaction Steps
2.0 g(0.0065 mol.) of ethyl 1,2-dimethyl-6-phenyl-4-oxonicotinate hydrochloride (see Example 49 below) is dissolved in water and treated with dilute sodium hydroxide (pH adjusted to about 8). The precipitate formed is isolated by vacuum filtration to afford 1.9 g of product, mp 154° C. (MDC/ether recrystallization).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04964896 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-c88888abae1e420c8ca8351d4f35c80b |
| Source note | uspto-grants-1990_10 |