反应详情

12.34 g (0.048 mol) of 2,4-dichlorophenacylimidazole and 6.66 g (0.05 mol) of cinnamylamine were suspended in 100 ml of toluene and the suspension was heated under reflux, using a water separator, until no further water of reaction was separated off. The solvent was removed in vacuo, after which 17.4 g (98% of theory) of a viscous oil were obtained.

1. temperaturethe suspension was heated
2. temperatureunder reflux
3. customwas separated off
4. customThe solvent was removed in vacuo
5. customafter which 17.4 g (98% of theory) of a viscous oil were obtained