HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86744308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 3-Phenylprop-2-en-1-amine | HCID 20369 | — |
| Reactant | 1-(2,4-dichlorophenyl)-2-(1H-imidazol-2-yl)ethanone | HCID 22142718 | — |
| Product | HCID 86744308 | HCID 86744308 | — |
Reaction Steps
12.34 g (0.048 mol) of 2,4-dichlorophenacylimidazole and 6.66 g (0.05 mol) of cinnamylamine were suspended in 100 ml of toluene and the suspension was heated under reflux, using a water separator, until no further water of reaction was separated off. The solvent was removed in vacuo, after which 17.4 g (98% of theory) of a viscous oil were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04965277 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-3b36f564aa4243c3847dff4e4017e7f0 |
| Source note | uspto-grants-1990_10 |