HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloroacetyl chloride → HCID 15713153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloroacetyl chloride | HCID 6593 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 15713151 | HCID 15713151 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 15713153 | HCID 15713153 | — |
Reaction Steps
In a similar manner as Example I, 27.7 milliliters of 25 percent w/v, 2,2-dimethyl-5-isopropoxymethyl oxazolidine solution in 50 milliliters of benzene and 4.9 grams of dichloroacetyl chloride was added 4.1 grams of triethylamine. After the appropriate work up procedure, there was obtained a yield of 8.9 grams, nD30 1.4564. Analytical data supports the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04965368 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-5baf44fb88254009bc0acf6883d38697 |
| Source note | uspto-grants-1990_10 |