HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22160874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 15713182 | HCID 15713182 | — |
| Reactant | HCID 22160872 | HCID 22160872 | — |
| Reactant | HCID 86744313 | HCID 86744313 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22160874 | HCID 22160874 | — |
Reaction Steps
To 19.3 milliliters of 25 percent w/v, 2,2-dimethyl-5-ethylthiomethyl oxazolidine solution in 25 milliliters of benzene was added 2.9 grams of triethylamine and 3.4 grams of ethylchlorothiolformate as in the procedure for (a) supra. Work-up was similar to (a). There was obtained a yield of 7.1 grams of the title compound, nD30 1.4940. Infrared data supports the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04965368 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-ba5bf78d942c4956ba801f625aee4be8 |
| Source note | uspto-grants-1990_10 |