HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → N-Benzyl-1-(methylsulfanyl)-2-nitroethen-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | HCID 11790510 | HCID 11790510 | — |
| Product | N-Benzyl-1-(methylsulfanyl)-2-nitroethen-1-amine | HCID 71391850 | — |
Reaction Steps
A mixture of nitromethane (4 ml), zeolite, RE 70 Na-Y (500 mg) and benzyl carbonimidodithioic acid dimethyl ester (XI, 500 mg) was refluxed for 110 hr. It was filtered and filtrate concentrated and treated with pet. ether. The solid that separated out was filtered and characterized as compound XII.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04967007 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-559a363de9d54431b4d93d6e60700340 |
| Source note | uspto-grants-1990_10 |