Diethyl Ether → HCID 19915455, compound

Participants

Reaction Conditions

Reaction Steps

54 g of 2-chloro-5-trifluoromethyl-1,3-dinitrobenzene are heated to 60° C. together with 64 g of ethylene glycolmonomethyl ether, and 23.5 g of 50 percent strength aqueous sodium hydroxide solution are added dropwise in the course of 30 minutes. The mixture is subsequently stirred at 60° C. for one hour, a further 5 g of sodium hydroxide solution are added and the mixture is subsequently stirred again at 60° C. for a further 1.5 hours. The mixture is then cooled, 50 ml of water are added and the product which has precipitated is filtered off and dried.

Provenance & Evidence