HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 10272356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | HCID 15023426 | HCID 15023426 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10272356 | HCID 10272356 | 64.8% |
Reaction Steps
A mixture of 3.1 g of 6-chloro-1-(phenylmethyl)benz[cd]indole-2(1H)-thione (Cr), 1.4 g of 1H-imidazole-1-propanamine, 250 ml of ethanol, 75 ml of dimethylformamide, and 3.5 g of mercuric acetate is reacted as described in Example 3, giving 2.6 g of the desired product, mp 147°-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079247 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-7618a83fdbfb4e7c808723756a35e711 |
| Source note | uspto-grants-1992_01 |