HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(1-Methylfluoren-9-yl)propionyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(1-Methylfluoren-9-yl)propionic acid | HCID 15045095 | — |
| Product | 3-(1-Methylfluoren-9-yl)propionyl Chloride | HCID 15045096 | — |
Reaction Steps
3-(1-Methylfluoren-9-yl)propionic acid (2.5 g, 9.9 mmol) was charged with SOCl2 (20 mL, in excess) at room temperature. The reaction mixture was boiled for 2 hr. Excess of thionyl chloride was removed under reduced pressure. The residual oil was used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079260 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-f72077c274bc48209040beb6f717b564 |
| Source note | uspto-grants-1992_01 |