HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodobenzoic acid → HCID 19978635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodobenzoic acid | HCID 6941 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Methyl-6-nitro-1H-indazole | HCID 10921054 | — |
| Catalyst | Copper oxide | HCID 14829 | — |
| Product | HCID 19978635 | HCID 19978635 | 97.2% |
Reaction Steps
3-Methyl-6-nitroindazole (64.5 g), 46.0 g of 2-iodobenzoic acid, 40.8 g of potassium carbonate and 1.89 g of copper(II) oxide were subjected to reaction in the same manner as in Example 1 to obtain 53.6 g (69.4%) of 1-(2-carboxyphenyl)-3-methyl-6-nitroindazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079358 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-e6d1e53a56084fdba1d677a616d1ec1b |
| Source note | uspto-grants-1992_01 |