HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14476647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14476646 | HCID 14476646 | — |
| Product | HCID 14476647 | HCID 14476647 | — |
Reaction Steps
76.8 g (0.336 mole) of 2-chloro 3-(1,1-dimethyl-2-hydroxy-ethyl)aminocarbonyl pyridine are placed in a reaction vessel immersed in a cooling bath (ice+water). 244 ml (3.36 moles) of thionyl chloride are then added so as to maintain the temperature below 20° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079363 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-40a48724a2094e74ae21538227fd5bec |
| Source note | uspto-grants-1992_01 |