HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,6,6-Tetramethylpiperidine → HCID 178418821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,6,6-Tetramethylpiperidine | HCID 13035 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 178418821 | HCID 178418821 | 100% |
Reaction Steps
A solution of 0.17 mole of lithium 2,2,6,6-tetramethyl piperidide is prepared by the addition of 0.17 mole of n-butyllithium (2.3 moles) in 74 ml of cyclohexane to 0.17 mole (28.7 ml) of 2,2,6,6-tetramethylpiperidine in 120 ml of tetrahydrofuran at a temperature below -20° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079363 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-3babfa32ffc340808c71308d40d3d4b6 |
| Source note | uspto-grants-1992_01 |