HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 19914186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 126244-29-9 | HCID 15692965 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19914186 | HCID 19914186 | — |
Reaction Steps
13.3 g of the carboxylic acid from Example b and 20 ml of thionyl chloride are refluxed in the presence of a little dimethylformamide until the evolution of gas is complete. The crude carbonyl chloride which remains in quantitative yield after evaporation is directly reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05080708 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-7cf12ad44771402099ffffb08370bb98 |
| Source note | uspto-grants-1992_01 |