HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 19914288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 12517819 | HCID 12517819 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 19914288 | HCID 19914288 | — |
Reaction Steps
To 2.5 g 10-amino-5,6-dihydro-11H-dibenzo(b,e)azepine-6,11-dione in 50 ml dioxane are added 2 ml anhydrous acetic acid. This mixture is kept at reflux for 2 hours then brought almost to dryness under reduced pressure, and then poured into water, filtered and dried. Yield 2 g (ethanol): melting point 270°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05080905 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-db376ed5bb294676b16b4b38595c2e99 |
| Source note | uspto-grants-1992_01 |