HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 9816434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 12517819 | HCID 12517819 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9816434 | HCID 9816434 | — |
Reaction Steps
To 5 g 10-amino-5,6-dihydro-11H-dibenzo(b,e)azepine-6,11-dione in 25 ml dimethylformamide are added 0.8 g 60% sodium hydride in mineral oil and then 1.5 ml methyl iodide. After leaving for 24 hours at ambient temperature, with stirring, the mixture is poured into water, filtered and dried: melting point 171°-3° C. (water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05080905 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-05b27af7e977488f8ee7693661efdd20 |
| Source note | uspto-grants-1992_01 |