HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 53684638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | (4-Methoxyphenyl)(2-methyl-3-nitrophenyl)methanone | HCID 14535915 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53684638 | HCID 53684638 | 91.9% |
Reaction Steps
A solution of 97.9 g (0.36 mole) of 3-(4-methoxybenzoyl)-2-methylnitrobenzene and 191 ml (1.45 mole) of DMF dimethyl acetal in 400 ml of DMF was heated under reflux for about nineteen hours and the reaction mixture then taken to dryness in vacuo to give 108 g of 2-(2-dimethylaminoethenyl)-3-(4-methoxybenzoyl)nitrobenzene as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081122 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-e179de2e60dd4e74833ea07d89a75eb0 |
| Source note | uspto-grants-1992_01 |