3-Methyl-5-oxoheptanoic acid → HCID 15678779, compound

HRID 1090191Notes

Reaction equation

HRID 1090191 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][N:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)N)=[CH:5][CH:4]=1.[CH3:20][CH:21]([CH2:26][C:27](=O)[CH2:28][CH3:29])[CH2:22][C:23]([OH:25])=[O:24]>C(O)(C)C>[CH3:20][CH:21]([CH2:26][C:27]1[N:10]([CH2:9][C:6]2[CH:7]=[CH:8][C:3]([Cl:2])=[CH:4][CH:5]=2)[C:12]2[C:17]([C:28]=1[CH3:29])=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)[CH2:22][C:23]([OH:25])=[O:24]

Participants

4

Reactant 2

HCID 156787783-Methyl-5-oxoheptanoic acidHCID 189475691-(4-Chlorobenzyl)-1-(4-methoxyphenyl)hydrazine hydrochloride

Product 1

HCID 15678779HCID 15678779, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Following the method of Example 2, but using 1-[(4-chlorophenyl)methyl]-1-(4-methoxyphenyl)hydrazine hydrochloride and 3-methyl-5-oxoheptanoic acid as the starting materials and isopropanol as the solvent, the title compound was prepared.

Sources & evidence

ORD record
ord-eacf4a0e26434788b070d282797d80f9
Source dataset
uspto-grants-1992_01
Patent number
US05081145

Reaction notes

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