HRID1090213

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13952862

3-(1H-Imidazol-1-yl)butan-1-amine

C7H13N3

结构：CN(C)S(=O)(=O)c1ccc2c3c(cccc13)C(=S)N2

HCID19914607

未命名化合物

PRODUCTS

生成物

结构：CC(CCNC1=Nc2ccc(S(=O)(=O)N(C)C)c3cccc1c23)n1ccnc1

HCID178448845

未命名化合物

收率 55.4%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 7.3 g of 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide, 4.2 g of 3-(1H-imidazol-l-yl)butanamine, 150 ml of ethanol and 9.6 g of mercuric acetate was reacted as described in Example 1, giving 5.5 g of the desired product, mp 221° C.-222° C.

WORKUP

后处理

customwas reacted