3-(1H-Imidazol-1-yl)butan-1-amine → HCID 178448845, compound

HRID 1090213Notes

Reaction equation

HRID 1090213 reaction equation
[CH3:1][N:2]([CH3:19])[S:3]([C:6]1[C:7]2[C:8]3[C:12](=[CH:13][CH:14]=1)[NH:11][C:10](=S)[C:9]=3[CH:16]=[CH:17][CH:18]=2)(=[O:5])=[O:4].[N:20]1([CH:25]([CH3:29])[CH2:26][CH2:27][NH2:28])[CH:24]=[CH:23][N:22]=[CH:21]1>C(O)C>[N:20]1([CH:25]([CH3:29])[CH2:26][CH2:27][NH:28][C:10]2[C:9]3[CH:16]=[CH:17][CH:18]=[C:7]4[C:8]=3[C:12](=[CH:13][CH:14]=[C:6]4[S:3]([N:2]([CH3:19])[CH3:1])(=[O:5])=[O:4])[N:11]=2)[CH:24]=[CH:23][N:22]=[CH:21]1

Participants

4

Reactant 2

HCID 139528623-(1H-Imidazol-1-yl)butan-1-amineHCID 199146071,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide

Product 1

HCID 178448845HCID 178448845, compoundYield 55.4%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 7.3 g of 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide, 4.2 g of 3-(1H-imidazol-l-yl)butanamine, 150 ml of ethanol and 9.6 g of mercuric acetate was reacted as described in Example 1, giving 5.5 g of the desired product, mp 221° C.-222° C.

Workup

  1. customwas reacted

Sources & evidence

ORD record
ord-1d77b605abee4ac281b5d4c8459fbbbf
Source dataset
uspto-grants-1992_01
Patent number
US05081131

Reaction notes

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