HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1H-Imidazol-1-yl)butan-1-amine → HCID 178448845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1H-Imidazol-1-yl)butan-1-amine | HCID 13952862 | — |
| Reactant | 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide | HCID 19914607 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178448845 | HCID 178448845 | 55.4% |
Reaction Steps
A mixture of 7.3 g of 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide, 4.2 g of 3-(1H-imidazol-l-yl)butanamine, 150 ml of ethanol and 9.6 g of mercuric acetate was reacted as described in Example 1, giving 5.5 g of the desired product, mp 221° C.-222° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081131 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-1d77b605abee4ac281b5d4c8459fbbbf |
| Source note | uspto-grants-1992_01 |