HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → Pyridine, 3-(4-aminobutyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | 5-Bromo-8-naphtholactam | HCID 754763 | — |
| Product | Pyridine, 3-(4-aminobutyl)- | HCID 72927 | — |
| Product | HCID 178527759 | HCID 178527759 | — |
Reaction Steps
4-(3-Pyridinyl)butylamine was prepared by the procedure described in Helv. Chim. Acta. 65 1868-1883 (1982). 6-Bromobenz(cd)indol-2-thiol was prepared by the action of P2S5 upon 6-bromobenz(cd)indol-2-one in refluxing pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081131 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-16cea23ece1a42acb1ada6a611c11f22 |
| Source note | uspto-grants-1992_01 |