HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 178448832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 3-(Pyridin-4-yl)butan-1-amine | HCID 14750817 | — |
| Reactant | HCID 178527764 | HCID 178527764 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178448832 | HCID 178448832 | — |
Reaction Steps
The title compound was prepared by the procedure of Example 55, utilizing 3.1 grams of 3-(4-pyridinyl)butanamine, 3.9 grams of benz(cd)indol-2-thiol, 6.4 grams of mercuric acetate, and 300 ml of ethanol. Chloroform (200 ml) was utilized as the partitioning solvent in place of dichloromethane. When the chloroform was being removed in vacuo, crystallization of the title compound suddenly occurred. The precipitate was collected, washed with a little chloroform, and dried. The yield was 3.9 grams; mp 220° C.-221° C. with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081131 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-93a06e6c415f427bb7b5418293efe56d |
| Source note | uspto-grants-1992_01 |