反应详情

A mixture consisting of 2.33 grams of 3-(1H-imidazol-1-yl)propoxyamine, 2.84 grams of benz(cd)indol-2-thiol, 4.9 grams of mercuric acetate, and 150 ml of ethanol as stirred and heated under reflux by the conditions of Example 55. The crude product was purified by the chromatographic procedure of Example 46. The resultant orange syrup was recrystallized from ethyl acetate-hexane to give 2.3 grams of the title compound; mp 102° C.-104° C.

1. temperatureheated
2. temperatureunder reflux by the conditions of Example 55
3. customThe crude product was purified by the chromatographic procedure of Example 46
4. customThe resultant orange syrup was recrystallized from ethyl acetate-hexane