HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1H-imidazol-1-yl)propoxyamine → N-(3-(1H-imidazol-1-yl)propoxy)benz(cd)indol-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1H-imidazol-1-yl)propoxyamine | HCID 15034994 | — |
| Reactant | HCID 178527764 | HCID 178527764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(3-(1H-imidazol-1-yl)propoxy)benz(cd)indol-2-amine | HCID 15035031 | 51.3% |
Reaction Steps
A mixture consisting of 2.33 grams of 3-(1H-imidazol-1-yl)propoxyamine, 2.84 grams of benz(cd)indol-2-thiol, 4.9 grams of mercuric acetate, and 150 ml of ethanol as stirred and heated under reflux by the conditions of Example 55. The crude product was purified by the chromatographic procedure of Example 46. The resultant orange syrup was recrystallized from ethyl acetate-hexane to give 2.3 grams of the title compound; mp 102° C.-104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081131 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-92e1a976caa8420f98fd3c40d235ddb5 |
| Source note | uspto-grants-1992_01 |