HCID 61699856, compound → HCID 178422608, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 2.6 grams of 4-(3-pryidinyl butylamine in 75 ml of ethanol, 5.1 grams of 8-methyl-2-methylthiobenz(cd)indole hydriodide was added. The mixture was then stirred and heated under reflux for 16 hours. The hot reaction mixture was clarified and the filtrate cooled at -10° C., yielding 4.75 grams of 8-methyl-N-(4-(3-pyridinyl)butyl)benz(cd)indol-2-amine hydriodide, m.p. 175°-176° C. with decomposition.

Provenance & Evidence