HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → HCID 14419664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Acetaldehyde, 2,2-dimethoxy- | HCID 162650 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14419664 | HCID 14419664 | — |
Reaction Steps
118 mmoles ethyl acrylate and 10 g (86.5 mmoles) of 90% by weight dimethoxyethanal in methanol were reacted using the method of example 1 to form 4,4-dimethoxy-2-ethoxycarbonyl-3-hydroxy-1-butene as a liquid which distilled at 108° C. under 0.3 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081276 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-82246b4ffff346a2aeccc9f5b4a05319 |
| Source note | uspto-grants-1992_01 |