Ethyl Acrylate → HCID 14419668, compound

HRID 1090359Notes

Reaction equation

HRID 1090359 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[CH2:8]([O:12][CH:13]([O:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:14]=[O:15])[CH2:9][CH2:10][CH3:11]>C(O)CCC>[CH2:17]([O:16][CH:13]([O:12][CH2:8][CH2:9][CH2:10][CH3:11])[CH:14]([OH:15])[C:2]([C:1]([O:5][CH2:6][CH3:7])=[O:4])=[CH2:3])[CH2:18][CH2:19][CH3:20]

Participants

4

Reactant 2

HCID 8821Ethyl AcrylateHCID 11084609HCID 11084609, compound

Product 1

HCID 14419668HCID 14419668, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

400 mmoles ethyl acrylate and 70 g (355 mmoles) of 95.5% by weight dibutoxyethanal in butanol were reacted using the method of example 1 to form 4,4-dibutoxy-2-ethoxycarbonyl-3-hydroxy-1-butene as a liquid which distilled at 120° C. under 0.4 mbar.

Sources & evidence

ORD record
ord-94d1818f85544109a687ee034202d9c3
Source dataset
uspto-grants-1992_01
Patent number
US05081276

Reaction notes

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