HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 178471864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 54318584 | HCID 54318584 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178471864 | HCID 178471864 | — |
Reaction Steps
A solution of 3.81 g (10 mmoles) of ethyl α-(ethoxymethylene)-2,5-difluoro-4-(1-methyl-4-piperidinyl)-β-oxobenzenepropanoate in 50 ml of ether was treated with 0.60 g (10 mmoles) of cyclopropylamine. After standing overnight the mixture was evaporated to dryness to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081254 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-f99075003c3447688ccbf7f87ba25ed6 |
| Source note | uspto-grants-1992_01 |