HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14623404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Reactant | HCID 14623403 | HCID 14623403 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14623404 | HCID 14623404 | — |
Reaction Steps
At room temperature, 1.1 g of triethylamine and then 1.0 g of cyclopropanecarboxylic acid chloride are dripped into 2.6 g of 2-[4-(6-chloropyridin-2-yloxy)-phenoxy]-ethylamine in 50 cm3 of dichloromethane. The reaction is slightly exothermic. The mixture is stirred at room temperature for 14 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082852 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-f60adf917b7f49ffabeee70105f5026a |
| Source note | uspto-grants-1992_01 |