HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 19762439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-(quinolin-2-ylmethoxy)benzoic Acid | HCID 9838552 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19762439 | HCID 19762439 | — |
Reaction Steps
1.28 g of 4-(quinolin-2-ylmethoxy)benzoic acid, in 4.6 ml of oxalyl chloride and 3 drops of dimethylformamide are combined in 50 ml of methylene chloride. The mixture is refluxed for 30 minutes and then concentrated in vacuo to give 4-(quinolin-2-ylmethoxy)benzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082849 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-1b31ef4038b04477b52cb80f4cdc673f |
| Source note | uspto-grants-1992_01 |