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HRID1090794

反应详情

EQUATION

反应方程式

HRID 1090794 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

结构：O=C(O)c1ccc(OCc2ccc3ccccc3n2)cc1
HCID9838552

4-(quinolin-2-ylmethoxy)benzoic Acid

C17H13NO3

PRODUCTS

生成物

1
结构：O=C(Cl)c1ccc(OCc2ccc3ccccc3n2)cc1
HCID19762439

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CN(C)C=O
催化剂HCID6228

N,N-Dimethylformamide

C3H7NO

结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

1.28 g of 4-(quinolin-2-ylmethoxy)benzoic acid, in 4.6 ml of oxalyl chloride and 3 drops of dimethylformamide are combined in 50 ml of methylene chloride. The mixture is refluxed for 30 minutes and then concentrated in vacuo to give 4-(quinolin-2-ylmethoxy)benzoyl chloride.

WORKUP

后处理

  1. temperatureThe mixture is refluxed for 30 minutes
  2. concentrationconcentrated in vacuo