Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Nitrotoluene | HCID 6944 | — |
| Reactant | HCID 86055794 | HCID 86055794 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67838982 | HCID 67838982 | — |
Reaction Steps
20.6 g of o-nitrotoluene of 24 g of bis-(dimethylamino) ethoxy methane in 50 ml of DMF were initially introduced into a distillation apparatus and the mixture was heated at 120° C. for 6 h to form the β-amino-2-nitrostyrene. The ethanol was then removed by briefly applying vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05082976 |
|---|
| Source dataset | uspto-grants-1992_01 |
|---|
| ORD ID | ord-03a4744d91fe4862bd5ea2128ea773de |
|---|
| Source note | uspto-grants-1992_01 |
|---|
