HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → 2-Nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | HCID 54256704 | HCID 54256704 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-Nitrobenzaldehyde | HCID 11101 | — |
Reaction Steps
50 mmol of β-morpholino-2-nitrostyrene and 1 g of CuCl were initially introduced into 120 ml of DMSO and aerated at 60° C. for 90 min. using oxygen. After concentrating and customary working-up, 0.41 mol of o-nitrobenzaldehyde was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082976 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-ef8e2d01f5f5496397b8c0fb5f24c393 |
| Source note | uspto-grants-1992_01 |