Hydrogen Peroxide → HCID 178522599, compound

Participants

Reaction Steps

To a stirred mixture of 4.5 g of the above benzamide in a mixture of 120 ml of methanolic ammonia plus 100 ml of methanol, was added dropwise, 3.6 ml of 30% hydrogen peroxide. This mixture was stirred overnight, the solid collected, partially dissolved in 500 ml of hot acetonitrile and filtered. The filtrate was chilled and the solid collected, giving 1.6 g of the desired product as white crystals, mp 227°-228° C. (dec.).

Provenance & Evidence