HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178423494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 2-[[(Benzoylamino)thioxomethyl)amino]-5-methylbenzamide | HCID 15135526 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178423494 | HCID 178423494 | 22.4% |
Reaction Steps
To a stirred mixture of 6 g of the above benzamide, 100 ml of methanolic ammonia and 200 ml of methanol was added dropwise, in increments, 20 ml of 30% hydrogen peroxide. After stirring overnight, the solid was collected, partially dissolved in 500 ml of hot acetonitrile and filtered. The filtrate was chilled, giving 1.2 g of the desired product as white crystals, mp 240°-242° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05084457 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-c542bc006b4445779e9a3dee954567a2 |
| Source note | uspto-grants-1992_01 |