HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 15135530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-4,5-dimethoxybenzamide | HCID 10867236 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15135530 | HCID 15135530 | 96.3% |
Reaction Steps
To a stirred mixture of 4 g of 2-amino-4,5-dimethoxybenzamide and 200 ml of ether was added dropwise, a solution of 3.3 g of benzoyl isothiocyanate in 100 ml of ether over 15 minutes. After 24 hours the solid was collected, giving 7 g of 2-[[(benzoylamino)thioxomethyl]amino]-4,5-dimethoxybenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05084457 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-1c547167972a442aa219695a14a7c01f |
| Source note | uspto-grants-1992_01 |