Ammonia → HCID 15027496, compound

Participants

Reaction Steps

To a stirred mixture of 6.6 g of the above benzamide, 100 ml of methanolic ammonia and 100 ml methanol was added, in increments, 20 ml of 30% hydrogen peroxide. After stirring overnight, the solid was collected, partially dissolved in 500 ml of hot acetonitrile and filtered. The filtrate was chilled, giving 1.5 g of the desired product as white crystals, mp 185°-186° C.

Provenance & Evidence