Acetonitrile → HCID 19913021, compound

Participants

Reaction Steps

A mixture of 0.61 g of 1,3-dimethyl-4-methylthio-5-nitro-1,2,3,6-tetrahydropyridylmethylamine, 0.357 g of 3 pyridylmethylamine and 6 ml of acetonitrile was stirred at room temperature for 5 hours. The reaction mixture was then concentrated and purified by column chromatography (eluent: dichloromethane-methanol (10:1)) to give 0.33 g of 1,3-dimethyl-4-(pyridylmethylamino)-5 nitro-1,2,3,6-tetrahydropyrimidine (Compound No. 31) as a syrup.

Provenance & Evidence